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| 气相色谱法测定水中呋喃丹 |
| Determ ination of Carbofunan in Water by Gas Chromatography |
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| DOI： |
| 中文关键词: 呋喃丹 毛细管 气相色谱法 水质 |
| 英文关键词: Carbofunan Capillary Gaschromatography Waterquality |
| 基金项目: |
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| 摘要点击次数: 1224 |
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| 中文摘要: |
| 建立了二氯甲烷提取、高效毛细管柱分离、气相色谱-氮磷检测器测定水中呋喃丹的方法。优化了试验条件, 以HP-5和HP-1301双柱定性, 方法在0.00 mg/L ～1.00 mg/L之间线性良好, 检出限为2.0 × 10 -5 mg/L,RSD ≤ 6.5% , 加标回收率为93.6% ～110% 。 |
| 英文摘要: |
| A method wasestablished fordetermination ofcarbofunanin watersamples which extracted with dichloromethane, separated byfused silicacapillarycolumn and detectedwith GC - NPD. Theexperimentcondi tion wasoptimized andthecompound decided by doublecapillarycolumns HP-5 and HP-1301. Thelinearre lation was excellent between instrumentresponds and calibration standard ranges both from 0. 00 mg/L to 1.00 mg/L. Thelimitsofdetectionin watersample were2.0 × 10 -5 mg/L. Therelative standard deviation waswithin 6.5% , and the recovery wasfrom 93.6% to110%. |
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