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固相萃取-高效液相色谱法测定水中磺酰脲类除草剂 |
Determ ination Sulphur Ureidein theW ater by SPE - HPLC |
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DOI: |
中文关键词: 固相萃取 高效液相色谱法 磺酰脲类除草剂 水质 |
英文关键词: Solid phaseextraction HPLC Sulphurureidesherbicides W aterquality |
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中文摘要: |
建立了固相萃取-高效液相色谱测定水中7种磺酰脲类除草剂的方法, 考察了降解作用及滤膜对测定的影响。方法在0.30 mg/L~ 5.00 m g/L之间线性关系良好,7 种磺酰脲类除草剂的检出限为0.32μg/L~ 0.62μ g/L, RSD为4.4% ~ 7.6%, 平均加标回收率为87.9% ~ 102% 。 |
英文摘要: |
Themethod wasestablished fordetermination of7 kindsofsulphurureidesherbicidesbysolid phaseextraction high effectiveliquid chromatography. Theinfluence ofdegradation action and filters were ob served. There were good linearrelationships between the instrumentalresponds and compoundsin range of 0.30mg/L and 5.00 mg/L ofthe method. The detectivelimitsof7 kindsofsulphur ureidesherbicides were 0.32μg/L~ 0.62μg/L, RSD 4.4% ~ 7.6%, avengerecoveries87.9% ~ 102%. |
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