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G C/MS法测定环境空气中痕量POPs类有机氯农药及降解产物 |
Determ ination of Trace Organo -Chlorine Pesticidesand Their DegradativeProductsin Ambient Air by GC /M S |
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DOI: |
中文关键词: 有机氯农药 降解产物 GC/MS 法 环境空气 |
英文关键词: Organo-chlorinepesticides Degradation product GC/MS Ambientair |
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中文摘要: |
采用快速溶剂萃取-氟罗里硅土柱净化-气相色谱/质谱联用法测定环境空气中 POPs 类有机氯农药及其降解产物。艾氏剂、狄氏剂、异狄氏剂、六六六、滴滴涕、七氯、氯丹、灭蚁灵及其降解产物的检出限为 2.0 ng ~4.6 ng,空白加标回收率为62.1% ~118% ,RSD为6.8% ~ 15.2% 。 |
英文摘要: |
A method wasestablished to determineorgano - chlorinepesticidesofPOPsand theirdegradative productsin the ambientairby accelerated solventextraction - florisilpurify-GC/MS. The detection limitsofdri nox, dieldrin, endrin, BHC, DDT, heptamul, chlordane, dechlorane and theirdegradativeproducts were from 2.0 ngto 4.6 ng. The blank recoveries were from 62.1% to118% and the RSD were from 6.8% to15.2%. |
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