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文章摘要
毛细管柱气相色谱法测定环境空气中的樟脑
Camphor Determination in Ambient Air by Capillary Gas Chromatography
  
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作者单位
王艳丽 天津市环境监测中心 
李利荣 天津市环境监测中心 
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中文摘要:
      采用毛细管柱气相色谱氢火焰离子化检测器测定环境空气中的樟脑,选择硅胶为吸附剂,甲醇/丙酮混合溶剂(体积比90∶10)为解析剂。方法在0.544 mg/L~109 mg/L范围内线性良好,检出限为0.06 mg/L,当采样体积为20 L时,最低检出质量浓度为0.003 mg/m3,标准溶液平行测定的RSD≤3.8%,空白加标回收率为95.4%~101%。
英文摘要:
      Camphor in the air was determined by gas chromatograph of capillary column with hydrogen flame ionization detector, using silica gel as adsorbent, and desorbed by mixed solvent [V(methanol)∶V(acetone)=90∶10]. Results of the method showed that good linearity was obtained in range from 0.544 mg/L to 109 mg/L, detection limit 0.06 mg/L, the lowest detection concentration 0.003 mg/m3 at sampling 20 liters air, RSD of standard solution≤3.8%, spiked recovery of blank from 95.4% to 101%.
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