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文章摘要
分光光度法测定水中硝基苯类化合物检出限的优化
The Optimization of Detection Limit for Determination of Nitrobenzene in Water by Spectrophotometric Method
  
DOI:
中文关键词: 硝基苯类化合物  锌还原-盐酸萘乙二胺分光光度法  检出限  水质
英文关键词: Nitrobenzene compounds  Zinc reduction-naphthyl ethylenediamine dihydrochloride spectrophotometric method  Detection limit  Water quality
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作者单位
丁建刚 泰兴市环境监测站 
黄桂荣 泰兴市环境监测站 
徐波 泰兴市环境监测站 
袁卫忠 泰兴市环境监测站 
刁小冬 泰兴市环境监测站 
田乐君 泰兴市环境监测站 
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中文摘要:
      对测定水中硝基苯类化合物的锌还原-盐酸萘乙二胺分光光度法进行优化,简化了操作步骤,并将参加显色反应的水样体积由4.0 mL增加至8.0 mL,比色皿厚度由10 mm增加至20 mm,方法推荐检出限由0.20 mg/L降至0.05 mg/L,实验室检出限为0.042 mg/L,改进后的方法对标准样品的测定结果符合要求。
英文摘要:
      The determination of nitrobenzene compounds by Zinc reduction-optimization-naphthyl-ethylenediamine-dihydrochloride spectrophotometric method was optimized. The operation steps were simplified, a water volume of 8.0 mL was used instead of 4.0 mL,a 20 mm cuvette was employed to take place of the 10 mm cuvette. The method detection limit decreased from recommended 0.20 mg/L to 0.05 mg/L. The laboratory detection limit was 0.042 mg/L. The determination results of standard sample meet the requirement by improved method.
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