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| 超声波提取-GC/MS法测定生物体内硝基苯类化合物 |
| Ultrasonic GC/MS Method for the Determination of Nitrobenzene Compounds in Biological Samples |
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| DOI： |
| 中文关键词: 硝基苯类化合物 超声波提取 凝胶色谱 气相色谱/质谱联用法 生物体 |
| 英文关键词: Nitrobenzene compounds Ultrasound Gel chromatography GC/MS Biology |
| 基金项目:2011年江苏省环境监测科研基金资助项目（1111） |
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| 中文摘要: |
| 以洪泽湖中6种代表性生物为研究对象，采用超声波法提取样品中硝基苯类化合物，用凝胶色谱净化、浓缩，气相色谱/质谱联用法测定。该法与索氏提取法在同等试验条件下进行加标回收试验，前者回收率高且稳定，简便可行。方法检出限为0.008 μg/g～0.030 μg/g，平均加标回收率为76.5%～109%，重复测定3次的RSD为1.5%～13.0%。 |
| 英文摘要: |
| Six representative biological samples from Hongze Lake were selected as researching objects. Nitrobenzene compounds in biological samples were extracted by ultrasonic extraction. Gel chromatography was applied to cleanup and concentration and quantification was done by GC/MS.Compared with the recoveries of the ultrasonic method and soxhlet extraction method under the same experimental conditions, the former method showed better recoveries and more stable.The detection limits were 0.008 μg/g～0.030 μg/g. The average spike recovery were from 76.5% to 109%, and the RSDs of three times repeated measurements were from 1.5% to 13.0%. |
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