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文章摘要
大气降水中钾钠钙镁测定方法的比对
Method Comparison of the Determination of K+, Na+, Ca2+,Mg2+ in Atmospheric Precipitation
  
DOI:
中文关键词:         原子吸收光谱法  电感耦合等离子体发射光谱法  离子色谱法  降水
英文关键词: K+  Na+  Ca2+  Mg2+  Atomic absorption spectrometry  Inductively coupled plasma atomic emission spectrometry  Ion chromatography  Precipitation
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作者单位
殷丽 上海市崇明县环境监测站 
张飞 上海市崇明县环境监测站 
唐溢湉 上海市崇明县环境监测站 
姜春燕 上海市崇明县环境监测站 
陈燕 上海市崇明县环境监测站 
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中文摘要:
      采用原子吸收光谱法(AAS)、电感耦合等离子体发射光谱法(ICP-AES)和离子色谱法(IC)分别测定降水中的钾、钠、钙、镁,对检出限、精密度、准确度和加标回收率等指标作比对,并对降水样品的测定结果进行t检验。结果表明,3种方法均能满足质量控制的要求,测定结果之间无显著性差异;与国标方法AAS法相比,ICP-AES法和IC法操作更简单,并可实现多元素的同时分析。
英文摘要:
      Atomic absorption spectrometry (AAS), inductively coupled plasma atomic emission spectrometry (ICP AES) and ion chromatography (IC) were used for determining the potassium, sodium, calcium and magnesium ions in precipitation.As compared to the detection limit, precision, accuracy and recovery rate, and the determination results of precipitation samples were analyzed by t test. The results showed that, the three methods could meet the requirement of quality control, there was no significant difference among the determination results. Compared with the national standard method of AAS, ICP AES method and IC method were more simple in operation and simultaneous determination of multiple elements were available.
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