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文章摘要
离子色谱法测定工作场所空气中二乙胺和三乙胺
Determination of Diethylamine and Triethylamine in Air of Workplace by Ion Chromatography
  
DOI:
中文关键词: 二乙胺  三乙胺  离子色谱法  工作场所空气
英文关键词: Diethylamine  Triethylamine  Ion chromatography  Air in workplace
基金项目:江苏省医学重点学科基金资助项目(ZDXK202249)
作者单位
沈菲 江苏省疾病预防控制中心 
谷静 江苏省疾病预防控制中心 
张昊 江苏省疾病预防控制中心 
朱宝立 江苏省疾病预防控制中心 
霍宗利 江苏省疾病预防控制中心 
朱醇 江苏省疾病预防控制中心 
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中文摘要:
      采用多孔玻板吸收管采集工作场所的空气,离子色谱法同时测定样品中的二乙胺和三乙胺。通过优化试验条件,使方法在0100mg/L~250mg/L范围内线性良好,二乙胺、三乙胺的方法检出限均为002mg/L。空白样品3个质量浓度水平的加标回收试验表明,二乙胺、三乙胺的加标回收率为968%~101%,6次测定结果的RSD为01%~19%。
英文摘要:
      Air in workplace was collected by porous glass plate absorption tube, and the contents of diethylamine and triethylamine in air samples were simultaneously determined by ion chromatography. By optimizing the test conditions,the method had good linearity in the range from 0.100 mg/L to 25.0 mg/L, and the detection limits of ethylamine and triethylamine were both 0.02 mg/L. The spiked recoveries of blank samples at three mass concentration levels of diethylamine and triethylamine were from 96.8% to 101%,and the RSDs of six measurements were from 0.1% to 1.9%.
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